Publication

NMSL Lab

Publication

Recycling of spent heat pack towards Fe-Fe3O4@ NC catalyst for ORR in direct methanol fuel cells and Al-air batteries
Author
Keyru Serbara Bejigo, Ruby Alphonse Raj, Sang-Jae Kim
Journal
Sustainable Materials and Technologies
Status
Volume 42
Page
e01153
Year
2024

Abstract

The effective repurposing of waste materials is crucial for sustainable development. The widespread use of disposable iron-based chemical warmers (IBCW) generates substantial solid waste annually. In this study, IBCWs were repurposed as raw materials to synthesize different electrocatalyst composites comprising metallic and oxide forms of iron embedded in nitrogen-doped carbon (NC). The composites were evaluated as oxygen reduction reaction (ORR) catalysts. The optimized Fe-Fe3O4@NC demonstrated enhanced ORR kinetics, with an onset potential of 0.92 V and a half-wave potential of 0.86 V vs. RHE. As an air cathode for direct methanol fuel cell (DMFC), Fe-Fe3O4@NC achieved a power density of 33.3 mW cm−2 at 88 mA cm−2, demonstrating its practical applicability. Additionally, a quasi solid-state aluminium-air battery (SAAB) was assembled using this catalyst as the air cathode with a PVA-KOH gel electrolyte and the separator. The quasi SAAB exhibited an open circuit voltage (OCV) of 1.46 V, a power density of 40 mW cm-2, and good rate capability compared to Pt/C. The combined effect of metallic and oxide iron with nitrogen doping enhances the overall catalytic activity. This study demonstrates that IBCWs can be effectively transformed into valuable catalysts for renewable energy applications, enabling clean and sustainable utilization of waste materials.
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